Application of high-performance liquid chromatography/high-resolution mass spectrometry to the investigation of sodium 2,3-disulfanyl-1-propanesulfonate (unithiol) and products of its oxidation with hydrogen peroxide
| Autor: | D. O. Kuleshov, S. V. Masyukevich, Z. A. Zhakovskaya, N. R. Gall, L. N. Gall, Y. V. Russkikh, T. E. Berezkina, Ekaterina Chernova |
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| Rok vydání: | 2016 |
| Předmět: |
0301 basic medicine
Chromatography Chemistry Sodium 010401 analytical chemistry chemistry.chemical_element Mass spectrometry 01 natural sciences High-performance liquid chromatography 0104 chemical sciences Analytical Chemistry 03 medical and health sciences chemistry.chemical_compound 030104 developmental biology Hydrogen peroxide |
| Zdroj: | Journal of Analytical Chemistry. 71:1381-1388 |
| ISSN: | 1608-3199 1061-9348 |
| DOI: | 10.1134/s1061934816140082 |
| Popis: | High-performance liquid chromatography combined with high-resolution mass spectrometry has been used to study the mild oxidation of sodium 2,3-disulfanyl-1-propanesulfonate (unithiol) with hydrogen peroxide. Reference peaks have been identified for the initial substance and reaction products. A possibility of using high-performance liquid chromatography with high-resolution mass spectrometry for the Sokolovskii thiol–disulphide test has been shown. |
| Databáze: | OpenAIRE |
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