Structural studies and physicochemical properties of l-valine hydrochloride monohydrate
Autor: | Tanusree Kar, Saikat Kumar Seth, Soma Adhikari |
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Rok vydání: | 2013 |
Předmět: |
Aqueous solution
Chemistry Hydrochloride Potassium Analytical chemistry chemistry.chemical_element Second-harmonic generation General Chemistry Crystal structure Condensed Matter Physics Evaporation (deposition) Crystal chemistry.chemical_compound Crystallography General Materials Science Single crystal |
Zdroj: | CrystEngComm. 15:7372 |
ISSN: | 1466-8033 |
DOI: | 10.1039/c3ce41079j |
Popis: | Nonlinear optical material L-valine hydrochloride monohydrate (VHM) was synthesized and single crystals were grown by slow evaporation of its aqueous solution at a constant temperature (42 °C). The crystal structure of VHM was redetermined by single crystal X-ray diffraction analysis. The physicochemical properties of the grown crystal were characterized by thermal and optical analysis and a measurement of hardness. The second harmonic generation efficiency of VHM was investigated by a powder method and it was found to be 0.3 times that of potassium dihydrogen phosphate (KDP). |
Databáze: | OpenAIRE |
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