Ultra-high resolution electron microscopy of defects in the CVD diamond structure

Autor: S. Delclos, François Silva, Alix Gicquel, D. Dorignac, F. Phillipp
Rok vydání: 1998
Předmět:
Zdroj: Diamond and Related Materials. 7:222-227
ISSN: 0925-9635
DOI: 10.1016/s0925-9635(97)00213-6
Popis: An elucidation of defect core structures in diamond thin films prepared by microwave plasma-assisted chemical vapour deposition (CVD) on silicon substrates is reported. The defects have been identified by ultra-high resolution electron microscopy (UHREM) at 0.15 nm resolution and associated image calculations. Three-dimensional atomic-scale models are proposed for three illustrative examples. The first two result from the interaction between a ∑ = 3 twin and (i) a perfect 60° dislocation and also (ii) a dissociated 0° dislocation. The last one (iii) consists of an original intrinsic stacking fault step. To our knowledge, it is the first time that such a type of defect has been reported. The experimental applicability of UHREM to the study of such complex defect configurations is also confirmed.
Databáze: OpenAIRE