Modification of Structural and Vibrational Properties of ZnO Nanoparticles Prepared by Simple Chemical Precipitation Method
| Autor: | Thutiyaporn Thiwawong, Benchapol Tunhoo, Natpasit Chaithanatkun, Korakot Onlaor |
|---|---|
| Rok vydání: | 2016 |
| Předmět: |
Materials science
Mechanical Engineering Inorganic chemistry Hexagonal phase Nanoparticle chemistry.chemical_element Zinc Field emission microscopy chemistry.chemical_compound Chemical engineering chemistry Mechanics of Materials Transmission electron microscopy Zinc nitrate Hydroxide General Materials Science Selected area diffraction |
| Zdroj: | Key Engineering Materials. :138-141 |
| ISSN: | 1662-9795 |
| DOI: | 10.4028/www.scientific.net/kem.675-676.138 |
| Popis: | In this work, zinc oxide (ZnO) nanoparticles were synthesized by simple chemical precipitation method in the present of zinc nitrate as zinc precursor and sodium hydroxide as hydroxide precursor. The vitamin C was used as modifier media to modify the structural properties of ZnO nanoparticles. The microstructures of ZnO nanoparticles were characterized by field emission scanning electron microscope (FE-SEM) and transmission electron microscope (TEM). Selected area electron diffraction (SAED) patterns showed that polycrystalline hexagonal phase of ZnO. The defects and impurity contents in nanoparticles were investigated by Fourier transform infrared (FT-IR) spectroscopy. The results show few carboxylate and hydroxyl impurities for larger particles when addition modifier increases. Surface areas of nanoparticles were measured by Brunauer Emmett Teller (BET) method. In addition, the results exhibited the dramatically change in structural properties of ZnO nanoparticles due to the effect of vitamin C. |
| Databáze: | OpenAIRE |
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