IMPLEMENTATION OF A DIFFERENTIAL PULSE ANODIC STRIPPING VOLTAMMETRY (DPASV) AT A HANGING MERCURY DROP ELECTRODE (HMDE) PROCEDURE FOR THE ANALYSIS OF AIRBORNE HEAVY METALS

Autor:	Eugenio O. Reyes-salas, José A. Manzanilla-Cano, Manuel H. Barceló-Quintal, J. Flores-Rodríguez
Rok vydání:	2001
Předmět:	Detection limit Cadmium Biochemistry (medical) Clinical Biochemistry Analytical chemistry chemistry.chemical_element Standard solution Biochemistry Analytical Chemistry law.invention Anodic stripping voltammetry chemistry law Hanging mercury drop electrode Standard addition Electrochemistry Inductively coupled plasma Atomic absorption spectroscopy Spectroscopy
Zdroj:	Analytical Letters. 34:2349-2360
ISSN:	1532-236X 0003-2719
DOI:	10.1081/al-100107300
Popis:	A procedure to determine cadmium, lead, zinc and copper in urban aerosol samples was developed. Differential-pulse anodic stripping voltammetry (DPASV) at a hanging mercury drop electrode (HMDE) was used as the analytical method, and accuracy of the procedure was checked using certified standard solutions. Metal concentrations were calculated from the corresponding regression line using the standard addition method; limits of detection of the four metals were also calculated. Detection and quantification of these metals by DPASV can substitute for other common techniques such as electrothermal atomic absorption spectrometry (EAAS) and inductively coupled plasma – atomic emission spectrometry (ICP-AES) as a confirmatory method.
Databáze:	OpenAIRE
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