Studies on electrochemical dissolution of sintered molybdenum discs as a potential method for targets dissolution in 99mTc production

Autor: Izabela Cieszykowska, Katarzyna Jerzyk, Małgorzata Żółtowska, Tomasz Janiak, Grażyna Birnbaum
Rok vydání: 2021
Předmět:
Zdroj: Journal of Radioanalytical and Nuclear Chemistry. 331:1029-1037
ISSN: 1588-2780
0236-5731
DOI: 10.1007/s10967-021-08155-3
Popis: Electrochemical dissolution of pressed into discs and sintered metallic molybdenum powder with the mass of 712 ± 10 mg (n = 15) in potassium hydroxide solution was studied in detail. The technique was considered to apply for dissolution of irradiated 100Mo target in the 99mTc production. The effect of various parameters, e.g., the concentration of the electrolyte solution, temperature, current density, and surface area of the platinum cathode, was investigated. The shortest time for total dissolution of molybdenum target was 70 min. This result was achieved using an electrolyte solution of 5 M KOH, temperature 55 °C and the current density of 365 mA/cm2.
Databáze: OpenAIRE