Microestimation of phosphate in the presence of large amounts of fluoride

Autor:	Walter Selig, Jack W. Frazer, Arthur M. Kray
Rok vydání:	1975
Předmět:	chemistry.chemical_compound Perchlorate chemistry Inorganic chemistry Potentiometric titration Electrode Titration Phosphate Reference electrode Fluoride Analytical Chemistry
Zdroj:	Mikrochimica Acta. 64:581-587
ISSN:	1436-5073 0026-3672
DOI:	10.1007/bf01219229
Popis:	A method for the microestimation of orthophosphate in the presence of large amounts of fluoride is described. A lead ion-selective electrode and a double-junction reference electrode are used to monitor the potentiometric titration with 0.01M lead perchlorate. Solutions are buffered at pH 8.25 to 8.75. A computer-controlled titration system is used for titration and data processing. Up to 400 mg of fluoride, a 13000-fold excess, can be tolerated in the estimation of 10−6 M phosphate.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::f05628d231765ac597ea5264c3ae3d78 https://doi.org/10.1007/bf01219229 Zobrazit plný text záznamu Full text from SpringerLink