Use of galvanostatic coulometry for determining nitroxoline
Autor: | Guzel Ziyatdinova, G. K. Budnikov, O. V. Shlyamina, S. G. Abdullina |
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Rok vydání: | 2007 |
Předmět: | |
Zdroj: | Journal of Analytical Chemistry. 62:957-959 |
ISSN: | 1608-3199 1061-9348 |
DOI: | 10.1134/s1061934807100103 |
Popis: | It was found that nitroxoline rapidly and quantitatively reacts with electrogenerated chlorine or bromine. The stoichiometric coefficients of these reactions are 1: 1.5 and 1: 1, respectively. The mechanism of the reaction of nitroxoline with electrogenerated bromine was proposed. A procedure was developed for the quantitative determination of nitroxoline in the substance and pharmaceuticals with a relative standard deviation of 1–3%. |
Databáze: | OpenAIRE |
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