Magic Angle Spinning without the Magic and Natural Abundance Matrix Isolation 13C NMR
Autor: | D. M. Grant, K. W. Zilm |
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Rok vydání: | 1979 |
Předmět: | |
Zdroj: | Magnetic Resonance and Related Phenomena ISBN: 9783642813467 |
DOI: | 10.1007/978-3-642-81344-3_33 |
Popis: | A novel magic angle sample spinner is described which overcomes the usual technical difficulties associated with MASS in such a way as to allow routine analysis of complex samples such as coal or gallstones with as little as 80 mg. Also, the first 13C cross polarization spectrum of a matrix isolated compound is reported. |
Databáze: | OpenAIRE |
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