Magic Angle Spinning without the Magic and Natural Abundance Matrix Isolation 13C NMR

Autor: D. M. Grant, K. W. Zilm
Rok vydání: 1979
Předmět:
Zdroj: Magnetic Resonance and Related Phenomena ISBN: 9783642813467
DOI: 10.1007/978-3-642-81344-3_33
Popis: A novel magic angle sample spinner is described which overcomes the usual technical difficulties associated with MASS in such a way as to allow routine analysis of complex samples such as coal or gallstones with as little as 80 mg. Also, the first 13C cross polarization spectrum of a matrix isolated compound is reported.
Databáze: OpenAIRE