Self-Organization of a Bioactive Nanostructured Oxide Layer at the Surface of Sintered Titanium Sponge Powder Subjected to Electrochemical Anodization
Autor: | A. I. Shelukhina, K. V. Stepanova, A. M. Shul’ga, N. M. Yakovleva, V. E. Tolstik, Alexander N. Kokatev |
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Rok vydání: | 2018 |
Předmět: |
Materials science
Physics and Astronomy (miscellaneous) Nanoporous Anodizing Scanning electron microscope Oxide 02 engineering and technology 010402 general chemistry 021001 nanoscience & nanotechnology 01 natural sciences 0104 chemical sciences Amorphous solid chemistry.chemical_compound chemistry Chemical engineering Surface modification 0210 nano-technology Porosity Layer (electronics) |
Zdroj: | Technical Physics. 63:1334-1340 |
ISSN: | 1090-6525 1063-7842 |
DOI: | 10.1134/s1063784218090062 |
Popis: | Self-ordered nanoporous/nanotubular oxide films are prepared on the surface of porous powder materials of a titanium sponge by electrochemical anodization. By using scanning electron and atomic force microscopies, we establish that anodization of sintered powder of a titanium sponge in an electrolyte containing H2SO4 (10%) and HF (0.15%) yields an X-ray amorphous TiO2 film with a thickness of 250–350 nm and a regular pattern of nanopores and nanotubes with diameters of 30 to 70 nm. Our results confirm that the described method for surface modification of sintered powders of a titanium sponge holds promise in manufacturing bioactive implants. |
Databáze: | OpenAIRE |
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