Rapid synthesis of Y3Al5O12 powders via plasma electrolysis
| Autor: | Yunjie Yang, Huanwu Cheng, Xiaolin Wei, Aiming Bu, Lin Lu, Yan Xiang, Weiwei Chen, Yongfu Zhang, Lu Wang, Maoyuan Li |
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| Rok vydání: | 2021 |
| Předmět: |
Diffraction
Electrolysis Materials science Scanning electron microscope Process Chemistry and Technology chemistry.chemical_element Yttrium Plasma Surfaces Coatings and Films Electronic Optical and Magnetic Materials Threshold voltage law.invention chemistry Chemical engineering law Aluminium Electrode Materials Chemistry Ceramics and Composites |
| Zdroj: | Ceramics International. 47:30147-30155 |
| ISSN: | 0272-8842 |
| DOI: | 10.1016/j.ceramint.2021.07.193 |
| Popis: | Yttrium aluminum garnet (Y3Al5O12, YAG) is an important functional material. However, the strict and complicated preparation has limited its wide application. This study aimed to rapidly synthesize Y3Al5O12 by plasma electrolysis for the first time. The prepared powder was studied from topography, structure and elements by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The powder had a good crystal form with a spherical shape. The single kind of diffraction peak of Y3Al5O12 in XRD revealed the high purity of the synthesized powders. The study of the relationship between the applied voltage and the synthesized powder revealed a threshold voltage of 210 V under the present condition. The higher voltage led to the damage of the electrode due to excessive heat. The synthesis of the YAG powder had a melt-quench process. The two processes were carried out at the same time. |
| Databáze: | OpenAIRE |
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