Effect of magnesium aluminum isopropoxide hydrolysis conditions on the properties of magnesium aluminate spinel powders
| Autor: | V. E. Vaganov, Stanislav Balabanov, V. V. Drobotenko, A. V. Fedin, E. M. Gavrishchuk, D. A. Permin |
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| Rok vydání: | 2014 |
| Předmět: |
Materials science
Magnesium General Chemical Engineering Inorganic chemistry Spinel Metals and Alloys chemistry.chemical_element engineering.material law.invention Inorganic Chemistry Hydrolysis chemistry.chemical_compound chemistry Chemical engineering law Aluminium Specific surface area Alkoxide Materials Chemistry engineering Calcination Particle size |
| Zdroj: | Inorganic Materials. 50:830-836 |
| ISSN: | 1608-3172 0020-1685 |
| DOI: | 10.1134/s0020168514080032 |
| Popis: | We have studied the influence of the conditions of hydrolysis of the magnesium aluminum double alkoxide MgAl2(OPr i )8 and the heating rate and calcination temperature of aluminum magnesium hydroxides on the particle size and morphology of magnesium aluminate spinel powders. Conditions of the two-step process have been identified that make it possible to reproducibly prepare MgAl2O4 nanopowders with controlled properties. We have obtained MgAl2O4 powders ranging in specific surface area from 2 to 160 m2/g. |
| Databáze: | OpenAIRE |
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