Mechanically activated solid-phase synthesis of copper(II), zinc(II), and cadmium(II) diethyldithiocarbamates
Autor: | V. D. Makhaev, L. A. Petrova |
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Rok vydání: | 2007 |
Předmět: | |
Zdroj: | Russian Journal of Inorganic Chemistry. 52:865-870 |
ISSN: | 1531-8613 0036-0236 |
DOI: | 10.1134/s0036023607060083 |
Popis: | The mechanically activated solid-phase reaction of copper, zinc, and cadmium chlorides with sodium diethyldithiocarbamate is studied. The course of the process and the extent of reaction are studied as affected by the parameters of the mechanical activation, subsequent heat treatment of the activated mixtures, and the nature of the reagents. Vacuum sublimation isolated zinc, copper, and cadmium diethyldithiocarbamates from mechanically activated mixtures. The extent of reaction reaches 97–99%. |
Databáze: | OpenAIRE |
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