Synthesis and X-ray diffraction data of 1-N-(4-pyridylmethyl)amino naphthalene

Autor:	Vladimir V. Kouznetsov, H. A. Camargo, José A. Henao, Diego F Amado
Rok vydání:	2010
Předmět:	Crystallography chemistry.chemical_compound Radiation Anhydrous ethanol Chemistry X-ray crystallography General Materials Science Condensed Matter Physics 4-pyridylmethyl Instrumentation Powder diffraction Monoclinic crystal system Naphthalene
Zdroj:	Powder Diffraction. 25:72-74
ISSN:	1945-7413 0885-7156
DOI:	10.1154/1.3302836
Popis:	1-N-(4-pyridylmethyl)amino naphtalene was synthesized by means of a reaction of alpha-naphthylamine, 4-pyridylcarboxyaldehyde, in anhydrous ethanol to obtainN-(4-pyridylen)-alpha-naphthylamine and that was reduced with NaBH4 to produce the wanted compound. The X-ray powder diffraction pattern for the new compound 1-N-(4-pyrydylmethyl)amino naphtalene was obtained. This compound crystallizes in a monoclinic system with refined unit cell parameters a=10.375(5) Å, b=17.665(6) Å, c=5.566(2) Å, β=100.11(3), and V=1004.3(5) Å3, with space group P2/m (No. 10).
Databáze:	OpenAIRE
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