Synthese, Kristallstruktur und Konformation von N-Acetyl-Cα,α-diethylglycin/Synthesis and Crystal Structure of N-Acetyl-Cα,α-diethylglycine

Autor:	Bernard Luciak, Adam S. Redlinski, Zdzisław Gałdecki, Miroslaw T. Leplawy, Krzysztof Kaczmarek
Rok vydání:	1992
Předmět:	Chemistry Stereochemistry General Chemistry Crystal structure
Zdroj:	Zeitschrift für Naturforschung B. 47:90-92
ISSN:	1865-7117 0932-0776
Popis:	The compound CH3-CO-NH-C(C2H5)2-COOH was synthesized from the corresponding free amino acid. N-Acetyl-Cα,α-diethylglycine crystallizes in the monoclinic space group P21/c with a = 13.551(2)Å, b = 11.110(3)Å, c = 13.569(3)Å, β = 111.54(2)°, Z = 8 , D = 1.21 g/cm3. This structure was solved by direct methods and refined to R = 0.084. N-Acetyl-Cα,α-diethylglycine shows a fully extended conformation in its -N H-C(C2H5)2-CO- part.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::e3cf9c88d3d60da3a9eddc545ac8dfbe https://doi.org/10.1515/znb-1992-0117 Zobrazit plný text záznamu