Synthesis of isotopically labelled 2-isopropylthioxanthone from 2,2′-dithiosalicylic acid and deuterium cumene

Autor:	Weicheng Yang, Kai Sun, Wang Haoran, Yang Chao, Yong Luo, Fang Chao
Rok vydání:	2016
Předmět:	Cumene Isopropylthioxanthone 010405 organic chemistry 010401 analytical chemistry Organic Chemistry Radiochemistry Natural abundance Deuterium labelled equipment and supplies Mass spectrometry 01 natural sciences Biochemistry 0104 chemical sciences Analytical Chemistry chemistry.chemical_compound chemistry Deuterium Drug Discovery Proton NMR Radiology Nuclear Medicine and imaging Dithiosalicylic acid Spectroscopy
Zdroj:	Journal of Labelled Compounds and Radiopharmaceuticals. 59:313-316
ISSN:	0362-4803
DOI:	10.1002/jlcr.3400
Popis:	Two efficient synthetic routes of stable deuterium labelled 2-isopropylthioxanthone were presented with 98.1% and 98.8% isotopic abundance in acceptable yields and excellent chemical purities. Their structures and the isotope-abundance were confirmed according to proton nuclear magnetic resonance and liquid chromatography-mass spectrometry.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::d8f8a65232ec9a02ad5132867f6e2ef2 https://doi.org/10.1002/jlcr.3400 Zobrazit plný text záznamu Plný text ve formátu PDF Plný text ve formátu HTML
Nepřihlášeným uživatelům se plný text nezobrazuje	K zobrazení výsledku je třeba se přihlásit.