The synthesis and purification of pentylenetetrazole-10-14C

Autor:	J. E. Christian, J. B. Data, J. F. Stiver
Rok vydání:	1970
Předmět:	Chromatography Organic Chemistry Liquid scintillation counting General Medicine Biochemistry Thin-layer chromatography Analytical Chemistry chemistry.chemical_compound chemistry Drug Discovery Hydrazoic acid Radiology Nuclear Medicine and imaging Sublimation (phase transition) Spectroscopy
Zdroj:	Journal of Labelled Compounds. 6:40-44
ISSN:	1099-1344 0022-2135
DOI:	10.1002/jlcr.2590060106
Popis:	Pentylenetrazole-10-14C was synthesized by reacting hydrazoic acid with cyclohexanone-1-14C. Purification was carried out using sublimation and thick layer chromatography. Proof of radiochemical purity was determined using thin layer chromatography and autoradiography. The specific activity was found using liquid scintillation counting.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::d7963c84627862560e961f6639f8aa32 https://doi.org/10.1002/jlcr.2590060106 Zobrazit plný text záznamu Plný text