Purification and characterization of the indicator calmagite

Autor: Robert B. Fulton, Byron Kratochvil, Frederick F. Cantwell, James Nolan
Rok vydání: 1981
Předmět:
Zdroj: Canadian Journal of Chemistry. 59:2539-2542
ISSN: 1480-3291
0008-4042
DOI: 10.1139/v81-365
Popis: A scheme for the purification of the azo dye calmagite is described which involves solvent extraction, column partition chromatography, and adsorption chromatography on a nonpolar adsorbent. The final product, analyzed by thin-layer chromatography and by acid–base and ion-pair titrations, is of >99% purity. Molar absorptivities and acid ionization constants are reported for the conjugate species.
Databáze: OpenAIRE