Purification and characterization of the indicator calmagite
Autor: | Robert B. Fulton, Byron Kratochvil, Frederick F. Cantwell, James Nolan |
---|---|
Rok vydání: | 1981 |
Předmět: | |
Zdroj: | Canadian Journal of Chemistry. 59:2539-2542 |
ISSN: | 1480-3291 0008-4042 |
DOI: | 10.1139/v81-365 |
Popis: | A scheme for the purification of the azo dye calmagite is described which involves solvent extraction, column partition chromatography, and adsorption chromatography on a nonpolar adsorbent. The final product, analyzed by thin-layer chromatography and by acid–base and ion-pair titrations, is of >99% purity. Molar absorptivities and acid ionization constants are reported for the conjugate species. |
Databáze: | OpenAIRE |
Externí odkaz: |