Preparation, single crystal growth and characterization of bis(tetrabutylammonium)bis(4,5-dithiolato-1,3-dithiole-2-thione)copper

Autor:	X.B. Sun, Xujiang Wang, W.F. Guo, X.Q. Hou, Quan Ren, H. Lü, Guanyun Zhang, Dongyu Xu
Rok vydání:	2007
Předmět:	Thermogravimetric analysis Infrared Chemistry chemistry.chemical_element Crystal growth General Chemistry Condensed Matter Physics Copper Crystallography Differential thermal analysis X-ray crystallography Physical chemistry General Materials Science Spectroscopy Powder diffraction
Zdroj:	Crystal Research and Technology. 42:349-355
ISSN:	1521-4079 0232-1300
DOI:	10.1002/crat.200610827
Popis:	The preparation and single crystal growth of bis(tetrabutylammonium)bis(4,5-dithiolato-1,3-dithiole-2-thione)copper, (I), are described. The energy gap Eg of (I) is about 2.38 eV. The nonlinear optical susceptibility χ(3) is about 1.3×10-3 esu at 1064 nm. The characterization of (I) has been performed by electronic absorption, infrared and X-ray powder diffraction spectroscopy. The thermal behavior of (I) has been investigated by means of thermogravimetric analysis (TGA) and differential thermal analysis (DTA) measurements in air. (© 2007 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim)
Databáze:	OpenAIRE
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