In situdynamic SEM imaging of hydration of cement using WETSEM technology
Autor: | Karen Scrivener, E. Gallucci |
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Rok vydání: | 2007 |
Předmět: | |
Zdroj: | Advances in Applied Ceramics. 106:319-326 |
ISSN: | 1743-6761 1743-6753 |
DOI: | 10.1179/174367607x228070 |
Popis: | This paper presents an in situ study of the hydration of cement pastes in the SEM, made possible by the development of a radical new technology for the investigation of wet samples: the QX capsule from QuantomiX, based on the WETSEM technology, consists of an electron transparent but water and air tight membrane, which allows the examination of cement/water suspensions without any further preparation. In this way the evolution of hydration can be followed dynamically - in the same sample - over time. Results obtained with this technique are described. In addition to plain water/cement pastes the impact of additives on the early formation of phases has been studied. The strengths and limitations of this technology were identified and discussed. |
Databáze: | OpenAIRE |
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