Reaction of bismuth nitrate with sodium citrate in water-glycerol solutions
Autor: | T. B. Kuvshinova, V. D. Volodin, V. M. Skorikov |
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Rok vydání: | 2009 |
Předmět: | |
Zdroj: | Russian Journal of Inorganic Chemistry. 54:1816-1819 |
ISSN: | 1531-8613 0036-0236 |
Popis: | The reaction in a Bi(NO3)3-Na3Hcit-(H2O + glycerol) system was studied in a wide range of component ratios by the solubility method and pH-metry in combination with chemical analysis of solid phases. Poorly soluble phases of Bi(Hcit)x(OH)3(1 − x) · mH2O (x < 1) and sodium bismuth citrate NaBiCit · 3H2O were obtained. The compounds synthesized were characterized, and their compositions were refined by X-ray diffraction, DTG, and IR spectroscopy. |
Databáze: | OpenAIRE |
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