Reaction of bismuth nitrate with sodium citrate in water-glycerol solutions

Autor: T. B. Kuvshinova, V. D. Volodin, V. M. Skorikov
Rok vydání: 2009
Předmět:
Zdroj: Russian Journal of Inorganic Chemistry. 54:1816-1819
ISSN: 1531-8613
0036-0236
Popis: The reaction in a Bi(NO3)3-Na3Hcit-(H2O + glycerol) system was studied in a wide range of component ratios by the solubility method and pH-metry in combination with chemical analysis of solid phases. Poorly soluble phases of Bi(Hcit)x(OH)3(1 − x) · mH2O (x < 1) and sodium bismuth citrate NaBiCit · 3H2O were obtained. The compounds synthesized were characterized, and their compositions were refined by X-ray diffraction, DTG, and IR spectroscopy.
Databáze: OpenAIRE