Phase formation in the BaCO3–PbO–Fe2O3–Nb2O5 system
Autor: | Yu. A. Lupitskaya, K. V. Abdrakhmanova, D. A. Kalganov |
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Rok vydání: | 2017 |
Předmět: |
Materials science
Rietveld refinement Scanning electron microscope Analytical chemistry Space group Mineralogy 02 engineering and technology 021001 nanoscience & nanotechnology 01 natural sciences Phase formation Surfaces Coatings and Films visual_art 0103 physical sciences visual_art.visual_art_medium Multiferroics Ceramic Thin film 010306 general physics 0210 nano-technology Solid solution |
Zdroj: | Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques. 11:87-91 |
ISSN: | 1819-7094 1027-4510 |
Popis: | Features of the formation of lead-ferroniobate compounds in the xBaCO3–(1 – x)PbO–Fe2O3–Nb2O5 system by solid-phase synthesis are investigated. For perovskite-type lead-ferroniobate solid solution, a single-phase concentration region is revealed at 1233 K. The crystalline structures of the synthesized compounds are refined using Rietveld analysis and the Pm3m and R3m space groups. Ceramic samples of lead ferroniobate are studied by scanning electron microscopy. |
Databáze: | OpenAIRE |
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