Autor: N. B. Sokolova, A. V. El'tsov, A. D. Grigor'ev, A. S. Shtol'vin, N. M. Dmitrieva
Rok vydání: 2002
Předmět:
Zdroj: Russian Journal of General Chemistry. 72:255-258
ISSN: 1070-3632
DOI: 10.1023/a:1015585820270
Popis: In a microwave field, phthalic anhydride reacts with p-chlorophenol to give 1,4-dihydroxyanthraquinone (quinizarin) within 10 min. The reaction with 4-chlorophthalic anhydride occurs similarly. Phthalic and chlorophthalic acids can be used instead of anhydrides. 3-Nitrophthalic acid and 3,4,5,6-tetrabromophthalic anhydride do not react with p-chlorophenol under these conditions.
Databáze: OpenAIRE