Autor: | N. B. Sokolova, A. V. El'tsov, A. D. Grigor'ev, A. S. Shtol'vin, N. M. Dmitrieva |
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Rok vydání: | 2002 |
Předmět: | |
Zdroj: | Russian Journal of General Chemistry. 72:255-258 |
ISSN: | 1070-3632 |
DOI: | 10.1023/a:1015585820270 |
Popis: | In a microwave field, phthalic anhydride reacts with p-chlorophenol to give 1,4-dihydroxyanthraquinone (quinizarin) within 10 min. The reaction with 4-chlorophthalic anhydride occurs similarly. Phthalic and chlorophthalic acids can be used instead of anhydrides. 3-Nitrophthalic acid and 3,4,5,6-tetrabromophthalic anhydride do not react with p-chlorophenol under these conditions. |
Databáze: | OpenAIRE |
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