Solid State Amorphization of Ti60Si40 Alloy via Mechanical Alloying
| Autor: | Jesús Cintas Físico, Raquel Astacio López, Petr Urban, Rosa M. Aranda Louvier, Fátima Ángela Ternero Fernández |
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| Rok vydání: | 2021 |
| Předmět: |
010302 applied physics
Materials science Silicon Mechanical Engineering Metallurgy Alloy Solid-state chemistry.chemical_element 02 engineering and technology engineering.material 021001 nanoscience & nanotechnology 01 natural sciences law.invention chemistry Mechanics of Materials law 0103 physical sciences engineering General Materials Science Crystallization 0210 nano-technology Titanium |
| Zdroj: | Key Engineering Materials. 876:7-12 |
| ISSN: | 1662-9795 |
| DOI: | 10.4028/www.scientific.net/kem.876.7 |
| Popis: | The effect of milling time on the microstructure evolution and formation of amorphous phase of Ti60Si40 alloy produced by mechanical alloying (MA) has been investigated. Laser diffraction, Scanning Electron Microscopy (SEM), X-ray Diffraction (XRD), Transmission Electron Microscopy (TEM) and Differential Scanning Calorimetry (DSC) were employed to characterize the particle size, morphology and structure of mechanically alloyed Ti60Si40. When the milling time is increased to 20 h, the particle size decreases from 23.7 to 4.7 μm, the shape of the particles changes to spherical and the crystalline structure is transformed into an amorphous phase. The amorphous Ti60Si40 alloy is stable when heating up to 750oC. Above this temperature, the cold crystallization of the intermetallic compounds Ti5Si3 and/or Ti5Si4 begins. |
| Databáze: | OpenAIRE |
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