1H- and 13C-nuclear magneticresonance spectra of rifampicin and 3-((dimethylhydrazono)methyl)rifamycin SV.thylhydrazono)methyl)rifamycin SV

Autor: Goro Tsukamoto, Masahiro Taguchi, Yukinobu Yamane, Norio Aikawa
Rok vydání: 1988
Předmět:
Zdroj: Chemical and Pharmaceutical Bulletin. 36:4157-4161
ISSN: 1347-5223
0009-2363
DOI: 10.1248/cpb.36.4157
Popis: Assignments of labile protons (NH, OH-1, OH-4 and OH-8) and naphthalene carbon atoms in the 1H-and 13C-nuclear magnetic resonance spectra of rifampicin (1) and 3-[(dimethylhydrazono)-methyl] rifamycin SV (2) in CDC13 were made based on long-range selective decoupling experiments. The published assignments of the labile protons and two naphthalene carbon atoms (C-5 and C-9) of 1 should be revised.
Databáze: OpenAIRE