Magnesium-vapor reduction of niobium oxide compounds

Autor: Kalinnikov Vladimir T, M. V. Kryzhanov, V. M. Orlov
Rok vydání: 2015
Předmět:
Zdroj: Doklady Chemistry. 465:257-260
ISSN: 1608-3113
0012-5008
DOI: 10.1134/s0012500815110026
Popis: The effect of precursor composition and reduction conditions on the characteristics of niobium powders obtained by magnesium reduction were studied. The hypothesis of the possible increase in the specific surface area of the powders by a large factor by using complex oxides as precursors was confirmed. With magnesium niobate Mg4Nb2O9 as the precursor, mesoporous powders, unprecedented in the world, with a specific surface area of up to150 m2 g–1 and an average pore size of 4.6 nm were produced.
Databáze: OpenAIRE