Synthesis of palladium nano-squares by polyol-hydrothermal method
| Autor: | Lulu Li, Long Chang Lv, Zhi Gang Wu, Zhi Min Ren |
|---|---|
| Rok vydání: | 2019 |
| Předmět: |
chemistry.chemical_classification
Aqueous solution Materials science chemistry.chemical_element 02 engineering and technology 010402 general chemistry 021001 nanoscience & nanotechnology 01 natural sciences Hydrothermal circulation 0104 chemical sciences Inorganic Chemistry chemistry.chemical_compound Chemical engineering chemistry Polyol Transmission electron microscopy Nano Materials Chemistry Physical and Theoretical Chemistry Selected area diffraction 0210 nano-technology Ethylene glycol Palladium |
| Zdroj: | Inorganic Chemistry Communications. 107:107498 |
| ISSN: | 1387-7003 |
| DOI: | 10.1016/j.inoche.2019.107498 |
| Popis: | The single crystalline palladium nano-squares with an average side length of ~10 nm were successfully prepared by using a one-step, one-pot polyol-hydrothermal process, in an aqueous mixture of PdCl2, ethylene glycol (EG), poly (vinyl pyrrolidone) and KBr. From the results of powder X-ray diffraction, transmission electron microscopy and selected area electron diffraction analyses, we confirm that the synthesized nano-squares are highly uniform in both size and shape containing (100) planes. The roles of PVP, KBr and EG in forming of palladium nano-squares were also studied. Compared with previous methods, the newly developed way is convenient, environment friendly and low-cost. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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