Improved carbon nanotube growth inside an anodic aluminum oxide template using microwave radiation
Autor: | Maryam Faraji, Sedigheh Dadras |
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Rok vydání: | 2018 |
Předmět: |
Materials science
Anodic Aluminum Oxide Scanning electron microscope 02 engineering and technology General Chemistry Carbon nanotube Radiation 010402 general chemistry 021001 nanoscience & nanotechnology Condensed Matter Physics 01 natural sciences 0104 chemical sciences law.invention chemistry.chemical_compound Ferrocene chemistry Chemical engineering law General Materials Science Graphite 0210 nano-technology Microwave |
Zdroj: | Journal of Physics and Chemistry of Solids. 116:203-208 |
ISSN: | 0022-3697 |
DOI: | 10.1016/j.jpcs.2018.01.039 |
Popis: | In this study, we achieved superfast growth of carbon nanotubes (CNTs) in an anodic aluminum oxide (AAO) template by applying microwave (MW) radiation. This is a simple and direct approach for growing CNTs using a MW oven. The CNTs were synthesized using MW radiation at a frequency of 2.45 GHz and power was applied at various levels of 900, 600, and 450 W. We used graphite and ferrocene in equal portions as precursors. The optimum conditions for the growth of CNTs inside a MW oven were a time period of 5 s and power of 450 W. In order to grow uniform CNTs, an AAO template was applied with the CNTs synthesized under optimum conditions. The morphology of the synthesized CNTs was investigated by scanning electron microscopy analysis. The average diameters of the CNTs obtained without the template were 22–27 nm, whereas the diameters of the CNTs prepared inside the AAO template were about 4–6 nm. |
Databáze: | OpenAIRE |
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