Determination of gallium in biological materials by electrothermal atomic absorption spectrometry

Autor: Hitomi Tsuchiya, Madoka Fujimori, Hirotake Orii, Kayoko Nakamura
Rok vydání: 1982
Předmět:
Zdroj: Analytica Chimica Acta. 138:129-136
ISSN: 0003-2670
DOI: 10.1016/s0003-2670(01)85295-8
Popis: In this determination of gallium, the condition of the graphite tubes influences the peak height. Common acids and salts seriously affect the results, but in the presence of EDTA, interferences of nitric and hydrochloric acids are suppressed completely, and interferences of phosphoric acid and some salts are suppressed partly. To compensate for the effects, a standard addition procedure is proposed, and is applied to healthy and tumor.bearing mice. A linear calibration is obtained for 0.12–12 ng Ga in 50-μl aliquots. The method is applied to tissues and body fluids with good recovery and precision.
Databáze: OpenAIRE