Comparative Study of Substituted LiMn[sub (2−x)]FexO[sub 4] via Sol-Gel Route

Autor:	A. F. M. Fadzil, N. S. A. Puada, R. H. Y. Subban, N. Kamarulzaman, Mohamad Rusop, Rihanum Yahaya Subban, Norlida Kamarulzaman, Wong Tin Wui
Rok vydání:	2010
Předmět:	Materials science Scanning electron microscope law Phase composition X-ray crystallography Analytical chemistry Calcination Particle size Cyclic voltammetry Stoichiometry Sol-gel Nuclear chemistry law.invention
Zdroj:	AIP Conference Proceedings.
ISSN:	0094-243X
DOI:	10.1063/1.3377840
Popis:	In this work, LiMn1.9Fe0.1O4 and LiMn1.5Fe0.5O4 were prepared by sol‐gel method according to proper stoichiometric ratio. It is then calcined at 850° C for 24 hours. Characterization studies of final products were done using XRD, FESEM, cyclic voltammetry (CV) and charge—discharge characteristics. Phase composition of the samples were studied from the XRD patterns obtained. For the microstructural studies, FESEM results show an average particle size of the bulk particles. From the charge—discharge characteristics, it showed that these samples exhibited good discharge capacities.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::c7b6ba598f19e66999534bfa2cb0ff85 https://doi.org/10.1063/1.3377840 Zobrazit plný text záznamu