Improvement in Flash Chromatography

Autor: Kazuhiro Maruyama, Sugiyama Haruhiko, Masami Fukumoto, Yoshitsugu Sakata, Yoshinori Naruta, Hitoshi Uemori
Rok vydání: 1988
Předmět:
Zdroj: Bulletin of the Chemical Society of Japan. 61:1815-1817
ISSN: 1348-0634
0009-2673
DOI: 10.1246/bcsj.61.1815
Popis: Optimum and higher resolution in flash chromatography (FC) has been realized with 20–40 μm silica gel, which gives 1.4–1.9 times larger theoretical plate numbers, than the reported one, 40–63 μm. A new FC tube is proposed and the combination of quartz-made chromatographic tube and silica gel with fluorescent indicator is conveniently used for the preparative separation of colorless but UV absorbing compounds.
Databáze: OpenAIRE