Improvement in Flash Chromatography
Autor: | Kazuhiro Maruyama, Sugiyama Haruhiko, Masami Fukumoto, Yoshitsugu Sakata, Yoshinori Naruta, Hitoshi Uemori |
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Rok vydání: | 1988 |
Předmět: | |
Zdroj: | Bulletin of the Chemical Society of Japan. 61:1815-1817 |
ISSN: | 1348-0634 0009-2673 |
DOI: | 10.1246/bcsj.61.1815 |
Popis: | Optimum and higher resolution in flash chromatography (FC) has been realized with 20–40 μm silica gel, which gives 1.4–1.9 times larger theoretical plate numbers, than the reported one, 40–63 μm. A new FC tube is proposed and the combination of quartz-made chromatographic tube and silica gel with fluorescent indicator is conveniently used for the preparative separation of colorless but UV absorbing compounds. |
Databáze: | OpenAIRE |
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