Role of polyethyleneimine (PEI) in synthesis of zinc oxide nanoparticles and their cytotoxicity effects
Autor: | K.D. Verma, Seyed Jamal Alavi, Majid Darroudi, Reza Kazemi Oskuee, Niloofar Khalili |
---|---|
Rok vydání: | 2015 |
Předmět: |
Materials science
Process Chemistry and Technology technology industry and agriculture Nanoparticle chemistry.chemical_element Zinc Surfaces Coatings and Films Electronic Optical and Magnetic Materials law.invention chemistry law Materials Chemistry Ceramics and Composites Organic chemistry Calcination Crystallite Fourier transform infrared spectroscopy Cytotoxicity Powder diffraction Wurtzite crystal structure Nuclear chemistry |
Zdroj: | Ceramics International. 41:10222-10226 |
ISSN: | 0272-8842 |
Popis: | Monodispersed zinc oxide nanoparticles (ZnO-NPs) were synthesized by a simple sol–gel method. In this process, polyethyleneimine (PEI) was used as a polymeric matrix and mild reaction conditions. The PEI acted as a stabilizing or capping agent and polymeric template for preparing ZnO-NPs. The ZnO-NPs were successfully grown at different calcination temperatures, and their crystallite structures were characterized using various methods, including TEM, PXRD, FTIR, and TGA/DTA techniques. The PXRD analysis revealed wurtzite hexagonal ZnO with preferential orientation at (101) reflection plane. Spherical ZnO-NPs were synthesized and its TEM image showed the formation of nanopowders in size of about 25 nm, while dose dependent toxicity with non-toxic effect of concentration below 6.25 µg/mL was observed in the studies of in vitro cytotoxicity on neuro2A cells. |
Databáze: | OpenAIRE |
Externí odkaz: |