Hydrothermal synthesis of silicon oxide clad uranium oxide nanowires
Autor: | Rita E. Hoggan, Jason M. Harp, Adrian R. Wagner, Kevin R. Tolman, Lingfeng He |
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Rok vydání: | 2017 |
Předmět: |
inorganic chemicals
Amorphous silicon Materials science technology industry and agriculture Nanowire Oxide 02 engineering and technology equipment and supplies 010402 general chemistry 021001 nanoscience & nanotechnology complex mixtures 01 natural sciences Hydrothermal circulation 0104 chemical sciences Nanomaterials stomatognathic diseases chemistry.chemical_compound chemistry Chemical engineering Materials Chemistry Ceramics and Composites Hydrothermal synthesis Uranium oxide 0210 nano-technology Silicon oxide |
Zdroj: | Journal of the American Ceramic Society. 101:1004-1008 |
ISSN: | 1551-2916 0002-7820 |
DOI: | 10.1111/jace.15295 |
Popis: | A facile method to synthesize silicon oxide clad uranium oxide nanowires is presented. U3Si2, used as a precursor, was oxidized to produce uranium oxide nanocrystallites and amorphous silicon oxide under hydrothermal conditions at 300°C and a pressure of 7.8 × 106 Pa. The growth of uranium oxide nanowires was assisted by silicon oxide via assembling the uranium oxide nanocrystallites in an amorphous silicon oxide matrix. The microstructure and composition of silicon oxide clad uranium oxide nanowires were characterized by XRD, SEM, TEM, and EDS. The uranium oxide in the nanowires was determined as UO2.34 with a fluoride cubic structure. |
Databáze: | OpenAIRE |
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