Polymer Films as Calibration Standards for X-ray Fluorescence Analysis
Autor: | H. Yasuda, T. G. Dzubay, P. J. Lamothe |
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Rok vydání: | 1976 |
Předmět: | |
Zdroj: | Advances in X-ray Analysis. 20:411-421 |
ISSN: | 2631-3626 0376-0308 |
DOI: | 10.1154/s0376030800012015 |
Popis: | A new type of calibration standard has been developed for X-ray fluorescence analysis of thin samples. Each standard consists of a polymer film containing a single calibration element. The film is cast from a homogeneous solution containing known amounts of an organometallic compound and a polymer. Polymers of cellulose acetate-propionate and polystyrene are used because of their low moisture affinity. The films have a low (2-4 mg/cm2) mass per unit area for minimal X-ray attenuation. Standards of V, Co, Hi, and Pb have been successfully made. Typical concentrations of 20 μg/cm2 yield excellent spectra with a low background. The method shows promise for making standards of additional elements. |
Databáze: | OpenAIRE |
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