Polymer Films as Calibration Standards for X-ray Fluorescence Analysis

Autor: H. Yasuda, T. G. Dzubay, P. J. Lamothe
Rok vydání: 1976
Předmět:
Zdroj: Advances in X-ray Analysis. 20:411-421
ISSN: 2631-3626
0376-0308
DOI: 10.1154/s0376030800012015
Popis: A new type of calibration standard has been developed for X-ray fluorescence analysis of thin samples. Each standard consists of a polymer film containing a single calibration element. The film is cast from a homogeneous solution containing known amounts of an organometallic compound and a polymer. Polymers of cellulose acetate-propionate and polystyrene are used because of their low moisture affinity. The films have a low (2-4 mg/cm2) mass per unit area for minimal X-ray attenuation. Standards of V, Co, Hi, and Pb have been successfully made. Typical concentrations of 20 μg/cm2 yield excellent spectra with a low background. The method shows promise for making standards of additional elements.
Databáze: OpenAIRE