Method Development and Determination of Chlorinated Polycyclic Aromatic Hydrocarbons in Different Matrices
| Autor: | Anja Lüth, Wolfgang Rotard, Carsten Schörnick, Birgit Wobst |
|---|---|
| Rok vydání: | 2021 |
| Předmět: |
Reproducibility
Analyte business.industry Extraction (chemistry) 04 agricultural and veterinary sciences 010501 environmental sciences 040401 food science 01 natural sciences Applied Microbiology and Biotechnology Method development Analytical Chemistry 0404 agricultural biotechnology Scientific method Environmental science Safety Risk Reliability and Quality Process engineering business Safety Research 0105 earth and related environmental sciences Food Science |
| Zdroj: | Food Analytical Methods. 14:1150-1166 |
| ISSN: | 1936-976X 1936-9751 |
| DOI: | 10.1007/s12161-020-01956-4 |
| Popis: | The aim of this study was to develop an analytical method, which separates selected chlorinated polycyclic aromatic hydrocarbons (Cl-PAHs) from fat, and fat-free or vegetable matrices. The method contains extraction-, cleanup-, and quantification steps. Integration of automated analysis actions, as in extraction and cleanup, should enhance the reproducibility, precision, and efficiency of the method. This was confirmed by validation of the overall analytical process. In the end, as a performance check, the developed method was applied on different matrices, e.g., tea, rice, grilled pork, and eel and predator eggs, as a non-food example. An inter-laboratory check was initiated as replacement for the lack of proficiency tests. Due to the high level of automation, both personnel and time effort are very low. In addition, the method is very robust with regard to the variability of the solvent selection and the loss of analytes by evaporation to dryness. It could be demonstrated that the developed method is applicable to different matrices with reproducible and precise results. This applies also to low-fat food and feed. |
| Databáze: | OpenAIRE |
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