Instant synthesis of gold nanoparticles at room temperature and SERS applications
Autor: | Eduardo Larios-Rodríguez, Ramón A.B. Alvarez, H. Arizpe-Chávez, R. Britto Hurtado, O. Rocha-Rocha, Y. Delgado-Beleño, M. Cortez-Valadez, C.E. Martinez-Nuñez, L. P. Ramírez-Rodríguez, M. Flores-Acosta, A. R. Hernández-Martínez |
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Rok vydání: | 2016 |
Předmět: |
Physics
Reducing agent Surface plasmon General Physics and Astronomy Nanoparticle Nanotechnology 02 engineering and technology Surface-enhanced Raman spectroscopy 010402 general chemistry 021001 nanoscience & nanotechnology 01 natural sciences 0104 chemical sciences Colloidal gold Transmission electron microscopy 0210 nano-technology Absorption (electromagnetic radiation) Plasmon |
Zdroj: | Physics Letters A. 380:2658-2663 |
ISSN: | 0375-9601 |
Popis: | Nowadays, gold nanoparticles (AuNps) can be used in a variety of applications, thus efficient methods to produce them are necessary. Several methods have been proposed in this area, but NPs production time is one limitation of these approaches. In this study, we propose a high competitive method to synthesize gold colloidal nanoparticles, instantaneously, using no-toxic reducing agents. These substances allow the instantaneous synthesis at room temperature, even without magnetic stirrers, ovens or ultrasonic baths. Optic analysis showed two absorption bands, associated with surface Plasmon as function of HAuCl 4 concentration. The nanoparticles synthesized have a 10–20 nm size, seen by the transmission electron microscopy (TEM). Therefore, it was possible to obtain several geometric patterns of AuNps, and the synthesis was performed reducing significantly processing time. Additionally, Mie and Fuchs theories were used to predict the location of the absorption bands linked to the plasmon surface in gold nanoparticles. The Surface Enhanced Raman Spectroscopy (SERS) effect was analyzed considering natural zeolite (Chabazite) as analyte, in order to determinate its possible application in soil analysis. |
Databáze: | OpenAIRE |
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