Structure of a new chelate complex MO2O3(dpm)4
| Autor: | Sofya B. Artemkina, P. A. Stabnikov, A. Yu. Ledneva, Vladimir E. Fedorov, L. V. Yanshole |
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| Rok vydání: | 2017 |
| Předmět: |
Thermogravimetric analysis
Materials science Infrared spectroscopy chemistry.chemical_element 02 engineering and technology Crystal structure Triclinic crystal system 021001 nanoscience & nanotechnology 010403 inorganic & nuclear chemistry 01 natural sciences 0104 chemical sciences Inorganic Chemistry Crystallography chemistry Molybdenum Materials Chemistry Mass spectrum Chelation Physical and Theoretical Chemistry 0210 nano-technology Thermal analysis |
| Zdroj: | Journal of Structural Chemistry. 58:758-762 |
| ISSN: | 1573-8779 0022-4766 |
| Popis: | A new Mo2O3(dpm)4 compound (I) is synthesized by the interaction of Mo(CO)6 with 2,2,6,6-tetramethylheptanedione-3,5 (dpm). The structure of complex I determined by the XRD method is as follows: triclinic crystal system, space group P–1, a = 10.1780(7) A, b = 10.1817(6) A, c = 13.3255(9) A, α = 110.562(2)°, β = 102.233(2)°, γ = 93.9041(19)°, V = 1248.17(14) A3. The compound is characterized by IR spectroscopy, mass-spectrometry and thermogravimetric analysis (TGA). |
| Databáze: | OpenAIRE |
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