Synthesis of Some Quaternary N-(1,4-anhydro-5-deoxy-D, L-ribitol-5-yl)ammonium Salts
Autor: | Sławomir Milewski, Artur Sikorski, Barbara Dmochowska, Izabela Łącka, Andrzej Wiśniewski, Eugenia Skorupa, Patrycja Świtecka |
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Rok vydání: | 2009 |
Předmět: | |
Zdroj: | Journal of Carbohydrate Chemistry. 28:222-233 |
ISSN: | 1532-2327 0732-8303 |
DOI: | 10.1080/07328300902887680 |
Popis: | The successful removal of the isopropylidene-protecting group from 1,4-anhydro-2,3-O-isopropylidene-5-O-tosyl-D,L-ribitol and from quaternary N-(1,4-anhydro-5-deoxy-2,3-O-isopropylidene-D,L-ribitol-5-yl)ammonium salts is reported. The structures of all isolates were determined by spectral analysis, including extensive 2-D NMR analyses. Single-crystal x-ray diffractions of 1,4-anhydro-5-O-tosyl-D,L-ribitol and its 2,3-O-isopropylidene derivatives are reported. |
Databáze: | OpenAIRE |
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