Fabrication and characterization of aluminum nitride sponges using a mixture of two porous formation methods
| Autor: | Raul Alejando Pulido Aguilar, José Egberto Bedolla Becerril, Carlos Arreola Fernandez, Rodrigo Alan Martínez Molina, Ena Athenea Aguilar Reyes |
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| Rok vydání: | 2019 |
| Předmět: |
Materials science
Mechanical Engineering Infrared spectroscopy 02 engineering and technology Thermal treatment Nitride 010402 general chemistry 021001 nanoscience & nanotechnology Condensed Matter Physics Microstructure 01 natural sciences 0104 chemical sciences Chemical engineering Mechanics of Materials visual_art Oxidizing agent visual_art.visual_art_medium General Materials Science Ceramic 0210 nano-technology Inert gas Porosity |
| Zdroj: | MRS Advances. 4:2977-2987 |
| ISSN: | 2059-8521 |
| Popis: | A method for the fabrication of interconnected ceramic sponges was used in the present work, designed by using a combination of two different, aqueous gel casting and sacrificial template, using aluminum nitride powder (99.97%) with a mean size of 2.4 micrometers. Two types of sponges were made by using two different monomers, acrylamide and methacrylamide, the resultants sponges have 60% of porosity after being sintered and pyrolyzed at temperature of 1673 K using an inert atmosphere of argon for 1 h. The hydrolysis evolution of this ceramic powder during the gelcasting process was studied by measuring the pH during the stirring time, the microstructure changes during the time of exposure were observed in a SEM. XRD were made to study the present phases after the gel was eliminated by thermal treatment at 873 K using an oxidizing atmosphere, observing a formation of up to 4 %wt. of cubic alumina phase which was made after the hydrolysis products. Infrared spectroscopy was used to study the changes in the ceramic powder. |
| Databáze: | OpenAIRE |
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