Facile Synthesis of ZnS Nanoparticles for Detection of O-nitrophenol
| Autor: | Yuanzhi Song, C. H. Lv, B. L. Dai, Jimin Xie, L. L. Zhang, Yong Ye |
|---|---|
| Rok vydání: | 2019 |
| Předmět: |
Materials science
Polymers and Plastics Scanning electron microscope Nanoparticle chemistry.chemical_element 02 engineering and technology Zinc 010402 general chemistry 021001 nanoscience & nanotechnology Electrochemistry 01 natural sciences 0104 chemical sciences Nitrophenol chemistry.chemical_compound chemistry Transmission electron microscopy Standard addition Materials Chemistry 0210 nano-technology Diffractometer Nuclear chemistry |
| Zdroj: | Journal of Inorganic and Organometallic Polymers and Materials. 30:1320-1326 |
| ISSN: | 1574-1451 1574-1443 |
| DOI: | 10.1007/s10904-019-01244-7 |
| Popis: | The ZnS nanoparticles were synthesized by hydrothermal method using thioacetamide and zinc chloride as precursors, and characterized by X-ray diffractometer, scanning electron microscopy, transmission electron microscopy, energy dispersive spectrometer and AC impedance spectroscopy. Electrochemical behavior of O-nitrophenol at nano ZnS modified glassy carbon electrode was investigated, and the reduction mechanism was discussed. Determination of artificial samples using the standard addition method was proposed, and recoveries were in the range from 96.3 to 102.0% with RSD of 1.3–2.0% (n = 6). |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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