Preparation of Aluminium dodecaboride (AlB12) powder by Self-propagating High-temperature Synthesis (SHS)

Autor: Lu Zhang, Xiaoming Cao, Xiangxin Xue, Chao Wang, Xiaozhou Cao, Jianxing Liu, Mengge Dong
Rok vydání: 2021
Předmět:
Zdroj: Open Journal of Chemistry. :025-028
ISSN: 2641-3051
DOI: 10.17352/ojc.000025
Popis: Self-propagating High-temperature Synthesis (SHS) process is used to prepare Aluminium dodecaboride (AlB12). The phase analysis results of preparing AlB12 with Al and B2O3 as raw materials show that under air and argon conditions, the self-propagating and acid-washed self-propagating powders all have α-Al2O3 impurities when Mg, Al and B2O3 are used as raw materials. The phase analysis results of the preparation of AlB12 show that under argon conditions, the self-propagating and acid-washed, self-propagating powder has un-removable MgAl2O4 impurities, and the root cause of the low purity of AlB12 prepared by the self-propagating method is the presence of un-removable impurities.
Databáze: OpenAIRE