Growth and characterization studies of an efficient semiorganic NLO single crystal: 2-Amino 5-Nitropyridinium Dihydrogen Phosphate (2A5NPDP) by Sankaranarayanan–Ramasamy method
| Autor: | Prem Anand Devarajan, M. Ambrose Rajkumar, S. Xavier, S. Anbarasu |
|---|---|
| Rok vydání: | 2016 |
| Předmět: |
010302 applied physics
Materials science 02 engineering and technology 021001 nanoscience & nanotechnology Phosphate 01 natural sciences Atomic and Molecular Physics and Optics Electronic Optical and Magnetic Materials Characterization (materials science) Crystal Crystallography chemistry.chemical_compound chemistry 0103 physical sciences Orthorhombic crystal system Electrical and Electronic Engineering Fourier transform infrared spectroscopy 0210 nano-technology Single crystal 2-amino-5-nitropyridinium dihydrogen phosphate Powder diffraction |
| Zdroj: | Optik. 127:2187-2192 |
| ISSN: | 0030-4026 |
| DOI: | 10.1016/j.ijleo.2015.10.239 |
| Popis: | An efficient semiorganic crystal of 2-Amino 5-Nitropyridinium Dihydrogen Phosphate (2A5NPDP) was grown using Sankaranarayanan–Ramasamy method. The presence of functional groups of 2-Amino 5-Nitropyridinium Dihyrogen Phosphate (2A5NPDP) was confirmed by FTIR analysis. Optical quality of the grown crystal was studied by UV–vis NIR analysis. Kurtz powder technique was used for NLO studies of the grown single crystal. The structure of 2-Amino 5-Nitropyridinium Dihydrogen Phosphate (2A5NPDP) was confirmed by single crystal XRD and XRPD analyses. TG/DTA studies revealed that the crystal was thermally stable up to179 °C. NMR and laser damage threshold analyses of 2-Amino 5-Nitropyridinium Dihydrogen Phosphate (2A5NPDP) studies also were carried out. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|
Full Text from ScienceDirect