An automatic adiabatic calorimeter for intermediate and high temperatures

Autor:	E. Sauerland, J. Helwig, H. E. Müser
Rok vydání:	1983
Předmět:	Phase transition Chemistry Thermistor Sapphire Analytical chemistry Calorimeter constant Physical and Theoretical Chemistry Atmospheric temperature range Condensed Matter Physics Adiabatic process Instrumentation Diode Calorimeter
Zdroj:	Thermochimica Acta. 69:253-267
ISSN:	0040-6031
DOI:	10.1016/0040-6031(83)85081-3
Popis:	A fully automated adiabatic calorimeter for a temperature range from 20 K to 670 K has been constructed. The system is used for specific heat measurements on solid state phase transitions with an absolute accuracy of 0.4 %. Usual temperature increments are 0.2 K or less per measuring cycle. The sample temperature is determined bv thermistors or diodes with a resolution of 0.1 mK. The whole measuring process is computer controlled: all received data are storedon data tape so that they can be easily evaluated. The performance of the apparatus is illustrated by results obtained on a sapphire sample.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::bc2c1edab7ccb55ce248723aa11bf674 https://doi.org/10.1016/0040-6031(83)85081-3 Zobrazit plný text záznamu