Enhanced acetone sensing performance of nanostructured Sm2O3 doped SnO2 thick films
| Autor: | J.Y. Patil, F.I. Shaikh, S.S. Suryavanshi, Imtiaz S. Mulla, L.P. Chikhale |
|---|---|
| Rok vydání: | 2017 |
| Předmět: |
Thermogravimetric analysis
Materials science Scanning electron microscope Doping Analytical chemistry 02 engineering and technology General Chemistry 010402 general chemistry 021001 nanoscience & nanotechnology 01 natural sciences 0104 chemical sciences Field electron emission chemistry.chemical_compound chemistry Geochemistry and Petrology Acetone Selected area diffraction 0210 nano-technology Selectivity Spectroscopy |
| Zdroj: | Journal of Rare Earths. 35:813-823 |
| ISSN: | 1002-0721 |
| DOI: | 10.1016/s1002-0721(17)60981-5 |
| Popis: | In the present work, we synthesized Sm 2 O 3 doped SnO 2 in order to prepare a selective acetone sensor with fast response, quick recovery and good repeatability. Pure as well as 2 mol.%, 4 mol.%, 6 mol.% and 8 mol.% Sm 2 O 3 doped SnO 2 nanostructured samples were synthesized by using a co-precipitation method. The characterization of the samples was done by thermogravimetric and differential thermo-gravimetric analysis (TG-DTA), X-ray diffraction (XRD), field emission gun-scanning electron microscopy (FEG-SEM), energy dispersive analysis by X-rays (EDAX), high resolution scanning electron microscopy (HR-TEM), selected area X-ray diffraction (SAED), Brunauer-Emmet-Teller (BET) and ultraviolet-visible-near infrared (UV-Vis-NIR) spectroscopy techniques. The gas response studies of liquid petroleum gas, ammonia, ethanol and acetone vapor were carried out. The results showed that Sm doping systematically lowered operating temperature and enhanced the gas response and selectivity for acetone. The response and recovery time for 6 mol.% Sm 2 O 3 doped SnO 2 thick film at the operating temperature of 250 °C were 15 and 24 s, respectively. |
| Databáze: | OpenAIRE |
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