Crystal Structure Analysis of a Hexatungstate by a High-Energy X-ray Diffraction Experiment Using an Imaging Plate Weissenberg Camera at the BL04B2 Beamline of SPring-8
Autor: | Maiko Isshiki, Shunsuke Oike, Hiroyuki Imura, Tomoji Ozeki, Noritaka Honma, Yuji Ohashi, Setsuko Nakamura, Nobuhiro Yasuda, Hidehiro Uekusa, Yuji Nakamura, Katsuhiro Kusaka, Chuji Katayama |
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Rok vydání: | 2001 |
Předmět: | |
Zdroj: | Chemistry Letters. 30:804-805 |
ISSN: | 1348-0715 0366-7022 |
Popis: | An imaging plate Weissenberg camera was installed in the BL04B2 beamline of SPring-8 aiming at automated crystal structure determinations of small molecules. Since this beamline is designed to provide X-rays with the energies higher than 37 keV (λ < 0.33 A), this camera is advantageous in crystal structure analyses of heavily X-ray absorbing materials. The title crystal structure analysis led to precise positional parameters and well-behaved displacement parameters not only for heavy atoms but also for light atoms. |
Databáze: | OpenAIRE |
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