Crystal Structure Analysis of a Hexatungstate by a High-Energy X-ray Diffraction Experiment Using an Imaging Plate Weissenberg Camera at the BL04B2 Beamline of SPring-8

Autor: Maiko Isshiki, Shunsuke Oike, Hiroyuki Imura, Tomoji Ozeki, Noritaka Honma, Yuji Ohashi, Setsuko Nakamura, Nobuhiro Yasuda, Hidehiro Uekusa, Yuji Nakamura, Katsuhiro Kusaka, Chuji Katayama
Rok vydání: 2001
Předmět:
Zdroj: Chemistry Letters. 30:804-805
ISSN: 1348-0715
0366-7022
Popis: An imaging plate Weissenberg camera was installed in the BL04B2 beamline of SPring-8 aiming at automated crystal structure determinations of small molecules. Since this beamline is designed to provide X-rays with the energies higher than 37 keV (λ < 0.33 A), this camera is advantageous in crystal structure analyses of heavily X-ray absorbing materials. The title crystal structure analysis led to precise positional parameters and well-behaved displacement parameters not only for heavy atoms but also for light atoms.
Databáze: OpenAIRE