Radiochemical separation of99Mo from natural uranium irradiated with thermal neutrons
Autor: | E. H. Abbas, H. A. Kaleefa, A. S. Al-Warith, M. A. A. Al-Janabi, M. G. Jalhoom |
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Rok vydání: | 1987 |
Předmět: |
Fission products
Nuclear fission product Elution Health Toxicology and Mutagenesis Radiochemistry Public Health Environmental and Occupational Health chemistry.chemical_element Natural uranium Uranium Pollution Analytical Chemistry Isotope separation law.invention chemistry.chemical_compound Nuclear Energy and Engineering chemistry Nitric acid law Radiology Nuclear Medicine and imaging Phosphoric acid Spectroscopy Nuclear chemistry |
Zdroj: | Journal of Radioanalytical and Nuclear Chemistry Articles. 111:165-175 |
ISSN: | 1588-2780 0236-5731 |
DOI: | 10.1007/bf02060533 |
Popis: | 99Mo was separated from uranium and insoluble fission product hydroxides. More than 98% of99Mo radioactivity was extracted with bis (2-ethylhexyl)phosphoric acid. The organic phase was washed and99Mo was back-extracted from the organic phase with NH4OH solution. The percent recovery from the organic phase was 91% and the purity of99Mo was more than 99%. Pure99mTc was also extracted from the organic phase with a saline solution. Reversed-phase partition chromatography was used for the purification of99Mo from131I and other fission products (10% HDEHP on kieselguhr bed).131I and other isotopes were quantitatively eluted with 0.1M H2SO4,99Mo was eluted using a mixture of 0.5 M HCl and 30% H2O2. |
Databáze: | OpenAIRE |
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