New tripodal ligand on the triphenylphosphine oxide platform with 1,2,3-triazole side arms: synthesis, structure, coordination, and extraction properties
| Autor: | Olga V. Bykhovskaya, Igor Yu. Kudryavtsev, Anna V. Vologzhanina, S. V. Matveev, Vasilii K. Karandashev, Valery K. Brel, Anna G. Matveeva, T. V. Baulina, Alexander N. Turanov, M. P. Pasechnik |
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| Rok vydání: | 2020 |
| Předmět: |
chemistry.chemical_classification
1 2 3-Triazole 010405 organic chemistry Aryl Triazole General Chemistry Nuclear magnetic resonance spectroscopy 010402 general chemistry 01 natural sciences 0104 chemical sciences chemistry.chemical_compound chemistry Tripodal ligand Polymer chemistry Click chemistry Alkyl Triphenylphosphine oxide |
| Zdroj: | Monatshefte für Chemie - Chemical Monthly. 151:1705-1713 |
| ISSN: | 1434-4475 0026-9247 |
| DOI: | 10.1007/s00706-020-02702-6 |
| Popis: | New hybrid tripodal propeller ligands on the triphenylphosphine oxide platform with triazole rings in the side arms and alkyl and aryl substituents in the triazole fragments have been synthesized by the click reaction. Composition and structure of the prepared compounds have been established by vibrational (IR, Raman) and multinuclear (1H, 13C, 31P) NMR spectroscopy, elemental analysis, and mass spectrometry. Coordination and extraction properties of the prepared compounds toward Pd(II) have been studied by the example of one of the ligands. |
| Databáze: | OpenAIRE |
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