A Facile and Convenient Method to Reduce Organo Azides under Electrochemical Condition and Investigation of the Process thorough Cyclic Voltammetry

Autor:	Paliakkara Lona Deena, Savariraj Joseph Selvaraj, Joby Thomas K
Rok vydání:	2022
Předmět:	Drug Discovery Environmental Chemistry General Chemistry Biochemistry
Zdroj:	Oriental Journal Of Chemistry. 38:1236-1243
ISSN:	2231-5039 0970-020X
DOI:	10.13005/ojc/380519
Popis:	Organo azides are potential precursors for the preparation of amines by different ways of chemical reduction. In the present studies , a simple and more convenient method was developed to reduce to the corresponding amine or sulphonamide under electrochemical condition using sodium ascorbate as the promoter and platinum electrodes. The reduction was achieved with sulfonyl azides, alkyl and aryl azides with moderate to quantitative yields. Cyclic voltametry studies were carried out to study this electrochemical reduction.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::b899850a7321b00e05f70ce5c72ccf50 https://doi.org/10.13005/ojc/380519 Zobrazit plný text záznamu