Crystal structure of tetraphenylarsonium nitridotetrachloroosmate(VI): a complex of five-coordinate osmium

Autor:	Frederick L. Phillips, Andrzej C. Skapski
Rok vydání:	1975
Předmět:	Tetragonal crystal system Crystallography chemistry.chemical_compound Structural Biology Chemistry chemistry.chemical_element Osmium General Chemistry Crystal structure Condensed Matter Physics Spectroscopy Organometallic chemistry Diffractometer
Zdroj:	Journal of Crystal and Molecular Structure. 5:83-92
ISSN:	1572-8854 0308-4086
DOI:	10.1007/bf01387002
Popis:	The crystal structure of tetraphenylarsonium nitridotetrachloroosmate(VI), (Ph4 As)[OsNCl4 ], has been determined from three-dimensional X-ray diffractometer data. The crystals are tetragonal with unit-cell dimensionsa = 12.667(3),c = 7.820(2) A, space groupP4/n andZ = 2. Full-matrix least-squares refinement, using 1189 independent reflections, has reachedR = 0.037.
Databáze:	OpenAIRE
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