On-line pressurized electromagnetic induction heating digestion: a promising sample preparation technique for trace mercury analysis

Autor:	Xianjuan Jiang, Hong-Jing Zi, Wu-Er Gan, Qing-De Su, Su-Ping Han
Rok vydání:	2008
Předmět:	Acid digestion Chromatography Chemistry Analytical chemistry chemistry.chemical_element Atomic fluorescence spectrometry Analytical Chemistry Electromagnetic induction Mercury (element) Cold vapor Sample preparation Cold vapour atomic fluorescence spectroscopy Spectroscopy Mercury analysis
Zdroj:	Journal of Analytical Atomic Spectrometry. 23:773
ISSN:	1364-5544 0267-9477
DOI:	10.1039/b717865d
Popis:	A novel, automated on-line pressurized sample digestion system based on electromagnetic induction heating technique was developed to perform solid sample decomposition in acid medium. The efficiency of acid digestion was increased with 0.36 MPa pressure built up in-line by a 0.5 mm id × 25 m length flow restrictor and up to approximately 135 °C reaction temperature. The system's performance was evaluated for on-line digestion of edible seaweeds and subsequent determination of mercury by cold vapor generation atomic fluorescence spectrometry (CVAFS).
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::b64a943472cca8162b9613d2502ced2b https://doi.org/10.1039/b717865d Zobrazit plný text záznamu